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https://hdl.handle.net/20.500.13091/4367
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DC Field | Value | Language |
---|---|---|
dc.contributor.author | Savkliyildiz, Ilyas | - |
dc.contributor.author | Degnah, Ahmed | - |
dc.contributor.author | Biçer, Hülya | - |
dc.contributor.author | Salur, Emin | - |
dc.contributor.author | Tsakalakos, Thomas | - |
dc.contributor.author | Akdoğan, Enver Koray | - |
dc.date.accessioned | 2023-08-03T19:00:16Z | - |
dc.date.available | 2023-08-03T19:00:16Z | - |
dc.date.issued | 2023 | - |
dc.identifier.issn | 0884-2914 | - |
dc.identifier.issn | 2044-5326 | - |
dc.identifier.uri | https://doi.org/10.1557/s43578-023-00910-4 | - |
dc.identifier.uri | https://hdl.handle.net/20.500.13091/4367 | - |
dc.description.abstract | High-energy synchrotron X-ray diffraction enables ultra-rapid data collection to determine unit cell volume evolution of 8YSZ under thermal and electric field (30 V/mm). Such an approach provides unprecedented insight into the anatomy of 8YSZ's flash sintering in the 797-810 & DEG;C interval. The densification due to flash sintering occurs in 40 s during which X-ray spectra were collected every 2 s. The densification of 8YSZ was accompanied by 0.55% anelastic peak shift on (220) reflection. Concomitantly, the applied thermal and electric field led to anelastic expansion of the cubic lattice parameter (+ 0.55%) and unit cell volume (+ 1.57%). Besides, an irreversible increase in the peak intensity (+ 22.6%), a decrease in peak width (- 18.3%), and integrated peak (- 13.6%) are determined. The observed anomalies are attributed to the response of oxygen vacancy generation and redistribution to the combined electric and thermal fields. | en_US |
dc.description.sponsorship | DOE Office of Science [DE-AC02-98CH10886] | en_US |
dc.description.sponsorship | The authors wish to thank Dr. Zhong Zhong (Brookhaven National Laboratory, Upton, NY, USA) for his valuable technical feedback. This research was accomplished in part at the National Synchrotron Light Source, a US Department of Energy (DOE) Office of Science User Facility operated for the DOE Office of Science by Brookhaven National Laboratory under Contract No. DE-AC02-98CH10886. | en_US |
dc.language.iso | en | en_US |
dc.publisher | Springer Heidelberg | en_US |
dc.relation.ispartof | Journal of Materials Research | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Unit cell expansion | en_US |
dc.subject | Synchrotron radiation | en_US |
dc.subject | YSZ | en_US |
dc.subject | Flash sintering | en_US |
dc.subject | Equation-Of-State | en_US |
dc.subject | Electric-Field | en_US |
dc.subject | Thermal Runaway | en_US |
dc.subject | Assisted Densification | en_US |
dc.subject | Lattice Expansion | en_US |
dc.subject | Temperature | en_US |
dc.subject | Microstructure | en_US |
dc.subject | Photoemission | en_US |
dc.subject | Model | en_US |
dc.subject | Onset | en_US |
dc.title | Anatomy of flash sintering in yttria-stabilized zirconia solid-state electrolyte: High temporal resolution energy-dispersive X-ray diffraction using a 200 keV synchrotron probe | en_US |
dc.type | Article | en_US |
dc.identifier.doi | 10.1557/s43578-023-00910-4 | - |
dc.identifier.scopus | 2-s2.0-85147349119 | en_US |
dc.department | KTÜN | en_US |
dc.authorid | Savkliyildiz, Ilyas/0000-0001-7903-9220 | - |
dc.identifier.volume | 38 | en_US |
dc.identifier.issue | 6 | en_US |
dc.identifier.startpage | 1583 | en_US |
dc.identifier.endpage | 1592 | en_US |
dc.identifier.wos | WOS:000925664300002 | en_US |
dc.institutionauthor | … | - |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.identifier.scopusquality | Q1 | - |
item.fulltext | No Fulltext | - |
item.openairetype | Article | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.grantfulltext | none | - |
item.cerifentitytype | Publications | - |
item.languageiso639-1 | en | - |
Appears in Collections: | Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collections WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collections |
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