Profile URL: https://hdl.handle.net/20.500.13091/11650
Job Title:Dr. Öğr. Üyesi
Email Address:hecevit@ktun.edu.tr
Main Affiliation:02.01. Department of Chemical Engineering
Status: Current Staff
ORCID:
0000-0003-0820-2064
0000-0003-0820-2064Scopus ID:
57217160554
57217160554YÖK Akademik: 2F3F2D3C3B2DCB52
Google Scholar:
pZFllmsAAAAJ
pZFllmsAAAAJWeb of Science ID:
A-9183-2019
A-9183-2019Name Variants:
Ecevit, H. Ecevit, Huseyin
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Article Citation - WoS: 2Citation - Scopus: 1Catalytic Degradation of Metronidazole by NaBH4 Reduction Using Ag/ Fe3O4-Bentonite Nanocomposite: Artificial Neural Network Modeling(Elsevier, 2025-08-01) Ecevit, Huseyin; Altun, TurkanIn this study, a novel ternary nanocomposite (Ag/Fe3O4-BNT) was developed by modifying bentonite with NaOH, incorporating magnetite nanoparticles (Fe3O4 NPs) via the solvothermal method, and subsequently incorporating silver nanoparticles (Ag NPs) through chemical precipitation. The synthesized nanocomposite was thoroughly characterized using point of zero charge measurement, Fourier transform infrared spectroscopy, Xray diffraction analysis, scanning electron microscopy coupled with energy dispersive X-ray spectroscopy, and thermogravimetric analysis techniques. Its catalytic activity was evaluated for the reduction of metronidazole (MNZ) antibiotic using sodium borohydride (NaBH4) as a reducing agent. Under optimized conditions (pH 7, 10 mM NaBH4, 0.25 g L-1 catalyst dosage, 30 mg L-1 MNZ, 25 degrees C), the system achieved 90 % MNZ removal within 90 min. An artificial neural network model was developed to predict removal efficiency based on experimental parameters, showing strong agreement with actual data. High-performance liquid chromatography analysis verified the formation of MNZ degradation products, and a possible degradation pathway was proposed. The combination of bentonite, Fe3O4, and Ag NPs demonstrated high catalytic activity, indicating its potential as an effective and magnetically separable catalyst for environmental applications.Article Citation - WoS: 34Citation - Scopus: 42Cr(vi) Removal Using Fe2o3-Chitosan Kernel Shell Pyrolytic Charcoal Composite Beads(KOREAN SOC ENVIRONMENTAL ENGINEERS, 2019-06-25) Altun, Türkan; Ecevit, HüseyinIn this study, cherry kernel shell pyrolytic charcoal was synthesized (CKSC) and composite beads were obtained by blending this pyrolytic charcoal with chitosan and Fe2O3 nanoparticles (Fe-C-CKSC). Cr(VI) adsorption from aqueous solutions by Fe-C-CKSC composite beads and CKSC adsorbents was studied comparatively. The effects of Cr(VI) initial concentration, adsorbent dosage, contact time, pH and temperature parameters on Cr(VI) adsorption were investigated. Adsorption reached an equilibrium point within 120 min for CKSC and Fe-C-CKSC adsorbents. The maximum Cr(VI) removal was obtained at the initial pH value of 1.56 for CKSC and 2.00 for Fe-C-CKSC. The optimum adsorbent dosage was found to be 5 g/L for CKSC and 3 g/L for Fe-C-CKSC. Based on the Langmuir model, the maximum adsorption capacities were calculated as 14.455 mg/g and 47.576 mg/g for CKSC and Fe-C-CKSC, respectively. Thermodynamic and kinetic studies were performed. As a result of adsorption kinetics calculations, adsorption was found to be consistent with the pseudo second order kinetic model. Characterization of the synthesized adsorbents was performed by SEM, BET, FTIR and elemental analysis. This study has shown that low cost adsorbents CKSC and Fe-C-CKSC can be used in Cr(VI) removal from aqueous solutions.Doctoral Thesis Gümüş Katkılı Manyetik Kil Nanokompozitleri Kullanılarak Metronidazol ve Siprofloksasin Antibiyotiklerinin Katalitik Bozunması ve Prosesin Yapay Sinir Ağları Yöntemiyle Modellenmesi(2024) Ecevit, Hüseyin; Altun, TürkanBu tez çalışmasında bentonit nanokili ve halloysit nanotüp kiline manyetik özellik kazandırmak amacıyla Fe3O4 nanoparçacıkları ve katalitik etkinliklerini artırmak için gümüş nanoparçacıkları katkılanmıştır. Bu şekilde elde edilen gümüş ve Fe3O4 nanoparçacıkları katkılı bentonit ve halloysit nanokompozitleri (Ag-FeBNT ve Ag-FeHNT) ile NaBH4 kullanılarak metronidazol ve siprofloksasin antibiyotiklerinin çözelti ortamından giderimi araştırılmıştır. Çalışmada, nanokompozitlerin adsorpsiyon kapasiteleri, yalnızca NaBH4 kullanılarak yapılan bozunma prosesinin verimliliği ve nanokompozitler ve NaBH4 kullanılarak gerçekleştirilen katalitik bozunma proseslerinin verimlilikleri karşılaştırılmıştır. Sonuçlar, adsorpsiyon ve katalizörsüz bozunma ile sınırlı bir giderim sağlanırken, katalitik bozunma süreçlerinin önemli ölçüde daha yüksek verimlilik sunduğunu göstermiştir. Nanokompozit sentezi sırasındaki aşamaların optimizasyonu için üretilen nanokompozitler ile antibiyotik giderim denemeleri yapılmış ve en verimli sonuçların elde edildiği gümüş katkılı manyetik kil nanokompozitleri sentezlenmiştir. Optimum sentez koşullarında elde edilen nanokompozitler çeşitli karakterizasyon yöntemleriyle incelenmiştir. Bu yöntemler arasında Fourier Dönüşümlü Kızılötesi Spektroskopisi, X-Işını Kırınımı, Taramalı Elektron Mikroskobu/Enerji Dağılımlı X-Işını Spektroskopisi, Termogravimetrik Analiz, Titreşimli Numune Manyetometresi, X-Işını Fotoelektron Spektroskopisi, Brunauer, Emmett ve Teller Yüzey Alanı Analizi, Sıfır Yük Noktası pH değeri ölçümleri yer almıştır. Daha sonra antibiyotiklerin gideriminde temas süresi, pH, NaBH4 derişimi, nanokompozit dozajı, antibiyotik derişimi ve sıcaklık parametrelerin etkileri değerlendirilmiş ve optimum giderim koşulları belirlenmiştir. Elde edilen sonuçlara göre, optimum koşullarda 90 dakikada metronidazolün Ag-FeBNT ile %90, Ag-FeHNT ile %89; siprofloksasinin ise Ag-FeBNT ile %85, Ag-FeHNT ile %82 oranında giderildiği bulunmuştur. Giderim proseslerinin modellenmesi yapay sinir ağları yöntemi kullanılarak gerçekleştirilmiş ve oluşturulan modelin prosesleri başarıyla temsil ettiği görülmüştür. Modelleme çalışmasında Ag-FeBNT ve Ag-FeHNT ile uygulanan giderim denemelerinin genel veri setlerine ait ortalama hata karesi değerleri, metronidazol giderimi için sırasıyla 0,0014 ve 0,0007; siprofloksasin giderimi için sırasıyla 0,0011 ve 0,0007 olarak bulunmuştur. Bu değerler, modelin süreçleri başarıyla temsil ettiğini göstermektedir. Son olarak, nanokompozitlerin katalitik bozunma proseslerinde geri dönüştürülebilirliği test edilmiş ve metronidazol gideriminde Ag-FeHNT'nin, siprofloksasin gideriminde ise her iki nanokompozitin de en az 6 kez kullanılabileceği gözlemlenmiştir. Ancak, Ag-FeBNT'nin metronidazol gideriminde ilk kullanım sonrası verim kaybettiği belirlenmiştir. Katalitik bozunma sonrası yapılan HPLC analizleri, metronidazol ve siprofloksasinin bozunmaya uğradığını kanıtlamış, ayrıca literatürdeki benzer çalışmalara dayanarak olası reaksiyon ürünleri raporlanmıştır.Article Citation - WoS: 10Citation - Scopus: 11Fabrication and Characterization of Halloysite–fe3o4–ag Nanocomposite as Efficient Catalyst for Metronidazole Degradation by Using Sodium Borohydride: Artificial Neural Network Modeling(Elsevier Ltd, 2024-04-01) Altun, T.; Ecevit, H.In this work, halloysite–Fe3O4–Ag nanocomposite produced by doping Fe3O4 and Ag nanoparticles on the surface of halloysite nanotube after activation with HCl by co-precipitation method was used as a catalyst for the catalytic degradation of metronidazole antibiotic with sodium borohydride. The physical and chemical structure of synthesized nanocomposite were characterized by pHpzc, FTIR, XRD, SEM/EDX and TGA. The degradation process of metronidazole antibiotic with sodium borohydride in the presence of nanocomposite catalyst was investigated. According to this, metronidazole removal efficiency was determined as %93.1 (as 0.069 in terms of Ct/C0) at the end of 120-min contact time under determined optimum conditions (pH 7, 10 mM NaBH4 concentration, 2 g/L catalyst dosage, 25 °C temperature) for 30 ppm metronidazole solution. In the pH range in which the process is applied, metronidazole is in anionic form in solution. The used nanocomposite was efficiently recycled and it was determined that it could be reused at least 6 times as a catalyst. Moreover, the process was modeled with Artificial Neural Networks approach. Finally, it was revealed with HPLC analysis that metronidazole was converted into different products as a result of applied process. © 2024 Elsevier B.V.Master Thesis Zirai Atık Kömüründen Elde Edilen Farklı Nanokompozitleri Kullanarak Sulu Çözeltilerden Cr(vı) Gideriminin İncelenmesi(Konya Teknik Üniversitesi, 2018) Ecevit, Hüseyin; Altun, TürkanAğır metallerin oluşturduğu su kirliliği, endüstriyel atıkların çevreye verdikleri zararların arasında önemli bir yer teşkil etmektedir. Atık sulardaki ağır metal kirliliğinin en önemli sebeplerinden birisi de, oldukça toksik bir iyon olan Cr(VI)'nın sulardaki varlığıdır. Bu tez çalışmasında hedeflenen; atık sulardan yüksek oranda Cr(VI) adsorpsiyonu kapasitesine sahip, doğal, ucuz ve kolay bulunabilen bir adsorban sentezini gerçekleştirmektir. Bu amaçla, vişne çekirdeği kabuğundan kömür (pirolitik çar) sentezlenmiştir. Sentezlenen vişne çekirdeği kabuğu pirolitik çarı (VÇKÇ) kullanılarak kompozit boncuklar elde edilmiş, sonrasında pirolitik çarın ve kompozit boncukların Cr(VI) adsorpsiyonunda kullanılabilirliği araştırılmıştır. Kompozit olarak vişne çekirdeği kabuğu pirolitik çarı/kitosan kompoziti (K-VÇKÇ) ve vişne çekirdeği kabuğu pirolitik çarı/kitosan/Fe2O3 nanokompoziti (Fe-K-VÇKÇ) hazırlanmıştır. Adsorbanların karakterizasyonları elementel analiz, FT-IR, SEM/EDX ve BET analizleri ile gerçekleştirilmiştir. Kesikli adsorpsiyon denemeleri ile adsorpsiyona etki eden; adsorban miktarı, konsantrasyon, pH, temas süresi, sıcaklık parametreleri optimize edilmiştir. Buna göre VÇKÇ, K-VÇKÇ ve Fe-K-VÇKÇ adsorbanları ile 55 mg/L'lik Cr(VI) çözeltisinden Cr(VI) adsorpsiyonu için optimum adsorban miktarları sırasıyla 5 g/L, 1,5 g/L ve 3 g/L olarak belirlenmiştir. Optimum temas süresi tüm adsorbanlar için 120 dk, optimum pH VÇKÇ için 1,56, K-VÇKÇ ve Fe-K-VÇKÇ için 2'dir. Sıcaklık artışının adsorpsiyonu arttırıcı yönde etkilediği; ancak bu artışın düşük düzeyde olduğu görülmüştür. Denge adsorpsiyon verileri kullanılarak Langmuir, Freundlich, Scatchard, Dubinin-Radushkevich ve Temkin izotermleri çizilmiş, bu izotermlerden adsorpsiyon parametreleri hesaplanmıştır. Adsorpsiyon Langmuir izotermine daha uyumlu bulunmuştur. Langmuir izotermi ile hesaplanan maksimum adsorpsiyon kapasiteleri VÇKÇ için 14,455 mg/g, K-VÇKÇ için 86,3 mg/g ve Fe-K-VÇKÇ için 47,576 mg/g'dır. Ayrıca kinetik hesaplamalar sonucunda adsorpsiyonun yalancı-ikinci mertebeden kinetik model ile uyumlu olduğu, termodinamik parametrelerin hesaplanması sonucunda da adsorpsiyonun istemli gerçekleştiği ve endotermik doğada olduğu belirlenmiştir.Article Citation - Scopus: 8Production of Chitosan Coated, Citric Acid Modified Almond, and Hazelnut Shell Adsorbents for Cr(vi) Removal and Investigation of Equilibrium, Kinetics, and Thermodynamics of Adsorption(SPRINGER HEIDELBERG, 2021-03-01) Altun, Türkan; Ecevit, Hüseyin; Çiftçi, BirsenRemoval of potentially toxic elements such as Cr(VI) from water bodies is crucial for health of aquatic organisms and human health. In order to produce an adsorbent with high Cr(VI) adsorption capacity, two different composite adsorbents were synthesized by coating citric acid modified almond and hazelnut shells with chitosan. Then, chitosan in the structure was cross-linked with glutaraldehyde. Cr(VI) adsorption performances of chitosan-citric acid modified almond shell composite (C-CA-AS) and chitosan-citric acid modified hazelnut shell composite (C-CA-HS) were investigated. The physical and chemical structures of the adsorbents before and after adsorption and chitosan coating were determined by Fourier transform infrared spectroscopy (FTIR), scanning electron microscope (SEM), and energy dispersive X-ray (EDX) analyses.Optimum adsorbent dosage, Cr(VI) concentration, pH, contact time, and temperature parameters were determined by batch adsorption experiments. Accordingly, the optimum adsorbent dosages for the adsorption of Cr(VI) from the 55 mg/L Cr(VI) solution using C-CA-AS and C-CA-HS adsorbents were 1.8 g/L and 1.0 g/L, respectively. For both adsorbents, the optimum contact time is 120 min; the optimum pH is 2.0. The increase in temperature enhanced the adsorption. Langmuir, Freundlich, Scatchard, Dubinin-Radushkevich, and Temkin isotherm graphs were drawn by using equilibrium adsorption data and the adsorption parameters were calculated from these isotherms. The adsorption equilibrium was found more compatible with Langmuir isotherm. The maximum adsorption capacities calculated by Langmuir isotherm were 100.3 mg/g for C-CA-AS and 89.5 mg/g for C-CA-HS. In addition, as a result of kinetic calculations, adsorption was found to be compatible with pseudo-second-order kinetic model, and as a result of calculation of thermodynamic parameters, it was determined that adsorption was spontaneous and endothermic. The data obtained in this study showed that the recommended adsorbents have higher adsorption capacities than many adsorbents described in the literature and commercial resins. In addition, since agricultural wastes are used in the adsorbents obtained, the adsorbents are low cost.Article Kitosan-vişne Çekirdeği Kabuğu Pirolitik Çarı Kompozit Boncuklarının Sentezi ve Karakterizasyonu: Cr(vı) Gideriminde Kullanılması(2019) Altun, Türkan; Ecevit, HüseyinBu çalışmada, vişne çekirdeği kabuğu pirolitik çarı (VÇKÇ) elde edilmiş ve bu pirolitik çarın kitosanla karıştırılarak boncukların oluşturulması yoluyla kitosan/pirolitik çar kompozit boncukları (K-VÇKÇ) sentezlenmiştir. Sonrasında VÇKÇ ve K-VÇKÇ boncuklarının sulu çözeltilerden Cr(VI) adsorpsiyonları karşılaştırmalı olarak incelenmiştir. Kesikli adsorpsiyon deneyleri sonucunda; Cr(VI) giderimi için optimum adsorban miktarı VÇKÇ için 5 g/L, K-VÇKÇ için ise 1,5 g/L; optimum pH VÇKÇ için 1,56, K-VÇKÇ için 2, optimum temas süresi 120 dk olarak belirlenmiştir. VÇKÇ ve K-VÇKÇ adsorbanları için adsorpsiyona, Langmuir İzoterm modelinin en uygun model olduğu görülmüştür. Bu izotermden, maksimum adsorpsiyon kapasiteleri VÇKÇ için 14,455 mg/g ve K-VÇKÇ için 86,298 mg/g olarak hesaplanmıştır. Termodinamik hesaplamalar, adsorpsiyonun endotermik ve istemli olduğunu göstermiştir. Adsorpsiyon kinetiği üzerine yapılan hesaplamalar sonucunda adsorpsiyonun yalancı ikinci mertebeden kinetik model ile uyumlu olduğu görülmüştür. Sentezlenen adsorbanların karakterizasyonu SEM/EDX, BET, FTIR ve elementel analiz ile gerçekleştirilmiştir. SEM/EDX ve FTIR analizleri ile Cr(VI)’nın adsorplandığı kanıtlanmıştır. Bu çalışma, VÇKÇ ve K-VÇKÇ’nin sulu çözeltilerden Cr(VI) gideriminde düşük maliyetli ve etkili bir adsorban olabileceğini göstermiştir.Article Citation - WoS: 42Citation - Scopus: 49Adsorption of Malachite Green and Methyl Violet 2b by Halloysite Nanotube: Batch Adsorption Experiments and Box-Behnken Experimental Design(Elsevier Ltd, 2022-11-01) Altun, Türkan; Ecevit, HüseyinDyes constitute a significant part of the pollutants in industrial wastewater. In this study, halloysite nanotube (HNT) was used for adsorption of malachite green and methyl violet 2B dyes from the solution. Using batch adsorption experiments and response surface method, parameters affecting adsorption have been optimized. As a consequence of the batch experiments, after 60 min, the adsorption equilibrium state was achieved at 3 g L?1 HNT dosage, 125 mg L?1 dye concentration and natural solution pH. Temperature did not significantly affect the adsorption. The adsorption equilibrium data can be said to have fitted the Langmuir, Freundlich, Dubinin-Radushkevich and Temkin isotherms well for the both dyes. The Langmuir maximum monolayer malachite green and methyl violet 2B adsorption capacities (As) of HNT are 74.95 mg g?1 and 67.87 mg g?1, respectively. Adsorption processes are more consistent with the pseudo-second-order kinetic model. In addition, both intra-particle diffusion and film diffusion are effective as rate-determining steps in adsorption. Thermodynamic calculations showed that the adsorption is exothermic and spontaneous. The regeneration of HNT after adsorption was confirmed in five cycles. By using the Box-Behnken response surface method, the parameters affecting the adsorption process were modeled, the effects of these parameters on the adsorption efficiency were expressed mathematically and the optimum operating parameters were determined. © 2022Article Citation - WoS: 1Modeling of Malachite Green Adsorption Onto Amberlite Irc-748 and Diaion Cr-11 Commercial Resins by Artificial Neural Network(Konya Teknik Univ, 2024-04-30) Ecevit, Hüseyin; Kola, Duygu Yanardag; Edebal, Serpil; Türkan Altun; Yanardag Kola, Duygu; Edebali, Serpil; Altun, TurkanIn this study, the malachite green adsorption process using Amberlite IRC-748 and Diaion CR-11 resins was modelled by artificial neural network method. In the model created for this study, adsorbent dosage, initial malachite green concentration and contact time parameters, which are the independent variables of the adsorption process, were used as input. Adsorption percentage values, which are the dependent variables of the adsorption process, were obtained as output. Mean squared error (MSE) and determination coefficient (R2) values were obtained from the models created using thirty-one experimental data for adsorption of malachite green with Amberlite IRC-748 and thirty-eight experimental data for adsorption with Diaion CR-11. By evaluating these values together, the most appropriate training algorithm, transfer function in the hidden layer and the number of neurons in the hidden layer were defined. Accordingly, for both Amberlite IRC-748 and Diaion CR-11 resins, the optimum training algorithm was determined as Levenberg-Marquardt back-propagation and the optimum hidden layer transfer function as tan sigmoid. The optimum number of neurons in the hidden layer was identified as 13 for Amberlite IRC-748 and 12 for Diaion CR11. The MSE, R2all and R2test values of the models produced with the optimum parameters were obtained as 0.000261, 0.9972, 0.9903 for Amberlite IRC-748 and 0.000482, 0.9932, 0.9931 for Diaion CR11, respectively.Article Citation - WoS: 18Citation - Scopus: 24Adsorption of Cr(vi) Onto Cross-Linked Chitosan-Almond Shell Biochars: Equilibrium, Kinetic, and Thermodynamic Studies(SPRINGER INTERNATIONAL PUBLISHING AG, 2021-08-19) Altun, Türkan; Ecevit, Hüseyin; Kar, Yakup; Çiftçi, BirsenIn this study, to remove Cr(VI) from the solution environment by adsorption, the almond shell was pyrolyzed at 400 and 500 degrees C and turned into biochar (ASC400 and ASC500) and composite adsorbents were obtained by coating these biochars with chitosan (Ch-ASC400 and Ch-ASC500). The resulting biochars and composite adsorbents were characterized using Fourier transform infrared (FTIR) spectroscopy; Brunauer, Emmett, and Teller (BET) surface area; scanning electron microscopy/energy-dispersive X-ray spectroscopy (SEM/EDX); and the point of zero charge pH (pH(pzc)) analyses. The parameters affecting the adsorption were examined with batch adsorption experiments and the optimum parameters for the efficient adsorption of Cr(VI) in 55 mg L-1 solution were determined as follows; adsorbent dosages: 5 g L-1 for biochars, 1.5 g L-1 for composite adsorbents, contact time: 120 min, pH: 1.5. It was seen that the temperature did not affect the adsorption much. Under optimum conditions, Cr(VI) adsorption capacities of ASC400, ASC500, Ch-ASC400, and Ch-ASC500 adsorbents are 11.33, 11.58, 37.48, and 36.65 mg g(-1), respectively, and their adsorption percentages are 95.2%, 97.5%, 94.3%, and 94.0%, respectively. Adsorption data were applied to Langmuir, Freundlich, Scatchard, Dubinin-Radushkevic, and Temkin isotherms and pseudo-first-order kinetic model, pseudo-second-order kinetic model, intra-particle diffusion model, and film diffusion model. The adsorption data fitted well to the Langmuir isotherm and pseudo-second-order kinetic models. From these results, it was determined that chemical adsorption is the dominant mechanism. Also, both intra-particle diffusion and film diffusion is effective in the adsorption rate. For all adsorbents, the Langmuir isotherm proved to be the most appropriate model for adsorption. The maximum monolayer adsorption capacities calculated from this model are 24.15 mg g(-1), 27.38 mg g(-1), 54.95 mg g(-1), and 87.86 mg g(-1) for ASC400, ASC500, Ch-ASC400, and Ch-ASC500, respectively. The enthalpy change, entropy change, and free energy changes during the adsorption process were calculated and the adsorption was also examined thermodynamically. As a result, adsorption occurs spontaneously for all adsorbents.
Research Topics
Domains
Physical Sciences
Fields
Environmental ScienceChemistryMaterials ScienceEnergy
Subfields
Water Science and TechnologyOrganic ChemistryBiomaterialsRenewable Energy, Sustainability and the EnvironmentAnalytical Chemistry
Specific Research Areas
Adsorption and biosorption for pollutant removal
Nanomaterials for catalytic reactions
Clay minerals and soil interactions
Iron oxide chemistry and applications
Analytical chemistry methods development
Sustainable Development Goals
6CLEAN WATER AND SANITATION
2
Research Products
11SUSTAINABLE CITIES AND COMMUNITIES
1
Research Products
14LIFE BELOW WATER
1
Research Products
Documents
6
Citations
135
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5
Documents
1
Citations
18
Publication Collaboration
| Affiliation Name | Count |
|---|---|
| Konya Technical University | 8 |
| Eskişehir Osmangazi University | 2 |
| İskenderun Technical University | 1 |
1 / 1
Data obtained from OpenAlex
| Journal | Count |
|---|---|
| Materials Chemistry and Physics | 2 |
| Çukurova Üniversitesi Mühendislik-Mimarlik Fakültesi Dergisi | 1 |
| ENVIRONMENTAL ENGINEERING RESEARCH | 1 |
| ARABIAN JOURNAL OF GEOSCIENCES | 1 |
| Journal of Water Process Engineering | 1 |
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107
Scopus Citation Count
135
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10.70
Scopus Citations per Publication
13.50
Open Access Source
5
Supervised Theses
2
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